Advanced GC Processes Troubleshooting And Control Systems

Code Date City Fees Register
T004 October 9, 2022 - October 13, 2022 Roma $ 5000

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T004 January 8, 2023 - January 12, 2023 Dubai – UAE $ 5000

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T004 April 9, 2023 - April 13, 2023 Istanbul $ 4500

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T004 July 9, 2023 - July 13, 2023 Online $ 1900

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Objectives

  • Upon Completion of the Course, Participants will be able to:
    • The aim is to provide first hand information to the participants on optimal use of gas chromatograph (GC).
    • A special emphasis has been given on the demonstration of applica­tions, maintenance and trouble­shooting of GC.
    • Imparting participants’ fundamen­tal knowledge of Gas Chromatog­raphy as a technique.
    • To understand GC maintenance methods as a routine checks.
    • Knowledge of accessories and con­sumables required for its opera­tion.
    • To familiarize participants to the techniques for achieving gas chro­matography analysis, qualitative and quantitative methods, cause and effect diagrams and standard curve.

The Delegates

  • All who works in any laboratory, i.e. clinical, industry, gas, petroleum, refinery, phar­macy, etc.
    • Laboratory manager and supervisor
    • Laboratory engineers and chemists
    • Laboratory analysts and technicians
    • Instrument engineers/technicians

The Contents

  • Theory Parameters:
    • Plate height(H),
    • Retention Time,
    • Capacity Fac­tor,
    • Selectivity Factor,
    • Column Efficiency,
    • Column Resolution.
  • Sampling And Sample Handling Iso 17025:
    • Requirements for Gases,
    • Liquid and Solid,
    • Sample Sampling Methods,
    • Sample Registra­tion and Storage,
    • Sample Disposal,
    • Max Holding Time of Sample,
    • Sample Contamination.
  • Sample Preparation And Analyte Manipulation Technique:
    • Solid-phase extraction,
    • Static head space technique,
    • Soxhlet extraction,
    • Microwave-assisted extraction,
    • Super critical fluid extraction
  • Derivatization Method:
    • Silyl,
    • Alkyl,
    • Acylation and Esterfication Methods
  • Types Of GC:
    • Normal GC,
    • High Speed GC and Portable GC
  • Gc Separation And Retention Process:
    • Dispersive Interac­tions,
    • Dipole-Dipole Interactions,
    • Dipole-Induced Dipole Interactions
  • Carrier Gas:
  • Van Deemter equation,
    • Optimal Practical Gas Velocity(OPGV),
    • Average Linear Velocity,
    • Flow Rate,
    • Carrier Gas Selection,
    • Pressure Regulator,
    • Gas Purification
  • Sample Injection System:
    • Sample Introduction Technique,
    • Manual Injection,
    • Solvent Flush Injection,
    • Septa,
    • Inlet Liner,
    • Split/Split less Inlets System,
    • Spit Ratio,
    • Purge Delay Time,
    • Cool On-Column Inlets,
    • Programmed Temperature Vaporization,
    • Headspace Technique,
    • Injection Problems,
    • Hot Vaporizing Injector
  • Column Configurations:
    • Stationary Phase of Packed and Capillary Column,
    • Packed Columns,
    • Temperature programming,
    • Gas-Liquid and Gas- Solid Columns,
    • Polarity and Selectivity,
    • Column Coating
  • Detectors:
    • Ideal Characteristics,
    • Column Position,
    • Gases,
    • Flame Ionization Detector,
    • Thermal Conductivity Detector,
    • Flame Photometric Detector,
    • Nitrogen Phosphorous Detector,
    • Photo Ionization Detector,
    • Electron Capture Detector,
    • Mass Spectrometry(Fragmentation and identify technique with software training),
    • Chemiluminescent Detector,
    • Mass Analyzer – Time of Flight,
    • Ion Trap and Quadrupole Technique.
  • Maintenance And Installation Methods:
    • Clean and Condition Septa,
    • Cleaning Injector Liners,
    • Silylating Liners,
    • Column Conditioning,
    • Installation Fused Silica Capillary Columns,
    • Column Placement in the oven,
    • Column Installation,
    • Leak Detection,
    • Bleed Test,
    • FidJet Cleaning Procedure,
    • TCD Clean Detector Cell,
    • Cleaning Of ECD,
    • FPD Mainte­nance,
    • Cleaning MS and Change The Filament
  • Instrument Problems And Troubleshooting:
    • Approaches to Solve GC Problems,
    • Troubleshooting Tests,
    • Band Broadening,
    • Broadening Initial Peak Band widths,
    • Retention Gap Sampling,
    • Sampling By Solute Fo­cusing,
    • Retention Gaps Tube,
    • Baseline Deviation,
    • Noisy Baseline,
    • Spikes in Baseline,
    • Peak Shape Problems,
    • Flat Top Peaks,
    • Split Peaks,
    • Negative Peaks,
    • Retention Changes,
    • Ghost Peak,
    • Causes and Prevention of Column Damage,
    • Column Contamination,
    • Needle Discrimination,
    • Change in Detec­tors Sensitivity,
    • Difficulty in Lighting Fid Flame,
    • Loss of Detectors Linear Range,
    • Leaks in MS,
    • Excessive Noise or High Background in MS
  • Practical Demonstration:
    • Introduction and familiarization with GC,
    • Preparation of sample test,
    • Preparation of standards,
    • Setting the methods program,
    • Inject the sample and standards,
    • Print the chromatograms,
    • Check all GC components and how to do the preventive maintenance
  • Quality Control And Validation Method:
    • Specificity,
    • Linear­ity,
    • Selectivity,
    • Accuracy,
    • Precision,
    • Bias,
    • Linearity,
    • Range,
    • Limit of De­tection,
    • Limit Of Quantification,
    • Robustness,
    • Ruggedness,
    • Stability
  • Quantitative Methods:
    • Interpolated Graph Calibration by Using External and Internal Standards,
    • Standard Addition Method,
    • Calibration Methods,
    • Correlation Coefficient,
    • Outliers Test of Repeated Measure­ments,
    • Outliers In Calibration Curve,
    • Errors In Quantitative Analysis,
    • Distribution of Errors,
    • Confidence Limit,
    • Limit of Detection,
    • Repeatabil­ity,
    • Reproducibility,
    • Optimization Methods
  • Course summary .

 Notes:

  • Great Discount for companies and governmental Organizations .
  • All programs are held in five star hotels .
  • All lecturers have sufficient knowledge and experience to implement the programs at an optimal level .
  • Large package of services is offered to the participants .

The Discount

10% in case of Three P. (or more)

Course File

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2024-01-03T07:41:22+00:00